Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
以苯

为原料,经
化,还原,环
等反

左旋西替利嗪盐酸盐,反
总收率为8.05%。
Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
以苯

为原料,经
化,还原,环
等反

左旋西替利嗪盐酸盐,反
总收率为8.05%。
Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘化钐在分子内环化反
中的
用。
Method The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.
方法以克拉霉素为起始原料,经水解、乙
化、环
酸酯化、氧化、脱
酸酯化、
化、环氨基
酸酯化和环
等反

目标化
物。
N butyl 2 ethoxy thioacridone was prepared from o chloro benzoic acid and p phenetidine by means of Ullman reaction,cyclization,N alkylation and sulfurization.
以邻
苯
酸和对乙氧基苯胺为原料,经过胺的苯基化、二芳胺的环化、N-烷基化、硫代化反

了N-丁基-2-乙氧基硫代吖啶酮。
This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.
讨论了以草酸二乙酯为原料,经过克莱森缩
、环
、氨解反

5
基异唑3
胺工艺的改进。
In this paper, the synthesis of 2 - chloranthraquinone and 2 - aminoanthraquinone was studied.It was prepared from phthalic anhydride by acetyiation, hydrolysis and cyclization.
以苯酐和取代苯为原料,经过乙
化、水解及环
反
,
了2-
蒽醌和2-氨基蒽醌,并对影响收率的工艺条件进行了研究。
Aqueous titanium trichloride promoted intermolecular reductive cyclization of 1,2 -diketone and o-nitroaniline in basic media provides a convenient method for the synthesis of quinoxaline derivatives.
本文研究了三
化钛水溶液作用下,邻硝基苯胺与1,2-二酮在碱性介质中分子间的
环反
,提供了一个方便地
取代喹喔啉类化
物的方法。
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